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Analysis of Organophosphorus-Based Nerve Agent Degradation Products by Gas Chromatography-Mass Spectrometry (GC-MS): Current Derivatization Reactions in the Analytical Chemist’s Toolbox

Molecules (Basel, Switzerland), 2021-07, Vol.26 (15), p.4631

2021

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Practical benzylation of N,N-substituted ethanolamines related to chemical warfare agents for analysis and detection by electron ionization gas chromatography-mass spectrometry

Journal of forensic sciences, 2023-11, Vol.68 (6), p.1923-1931

2023

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Trimethyloxonium-mediated methylation strategies for the rapid and simultaneous analysis of chlorinated phenols in various soils by electron impact gas chromatography-mass spectrometry

Scientific reports, 2022-01, Vol.12 (1), p.1401-1401, Article 1401

2022

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Analysis, identification and confirmation of synthetic opioids using chloroformate chemistry: Retrospective detection of fentanyl and acetylfentanyl in urine and plasma samples by EI-GC-MS and HR-LC-MS

PloS one, 2022-11, Vol.17 (11), p.e0275931-e0275931

2022

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Benzyl trichloroacetimidates as derivatizing agents for phosphonic acids related to nerve agents by EI-GC-MS during OPCW proficiency test scenarios

Scientific reports, 2022-12, Vol.12 (1), p.21299-11, Article 21299

2022

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An efficient, optimized synthesis of fentanyl and related analogs

PloS one, 2014-09, Vol.9 (9), p.e108250-e108250

2014

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Evaluation of polyanionic cyclodextrins as high affinity binding scaffolds for fentanyl

Scientific reports, 2023-02, Vol.13 (1), p.2680-2680, Article 2680

2023

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Evaluation of 6-OxP-CD, an Oxime-based cyclodextrin as a viable medical countermeasure against nerve agent poisoning: Experimental and molecular dynamic simulation studies on its inclusion complexes with cyclosarin, soman and VX

PloS one, 2023-03, Vol.18 (3), p.e0283181-e0283181

2023

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Analysis of chemical warfare agents by gas chromatography-mass spectrometry: methods for their direct detection and derivatization approaches for the analysis of their degradation products

Reviews in analytical chemistry, 2018-03, Vol.37 (1), p.3936-3942

2018

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Structural modification of fentanyls for their retrospective identification by gas chromatographic analysis using chloroformate chemistry

Scientific reports, 2021-11, Vol.11 (1), p.22489-22489, Article 22489

2021

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Gas Chromatography-Mass Spectrometry Analysis of Synthetic Opioids Belonging to the Fentanyl Class: A Review

Critical reviews in analytical chemistry, 2022, Vol.52 (8), p.1938-1968

Valdez, Carlos A.

2022

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Development of a CNS-permeable reactivator for nerve agent exposure: an iterative, multi-disciplinary approach

Scientific reports, 2021-07, Vol.11 (1), p.15567-16, Article 15567

2021

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Dose-dependent consequences of sub-chronic fentanyl exposure on neuron and glial co-cultures

Frontiers in toxicology, 2022-08, Vol.4, p.983415-983415

2022

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Predicting a Drug’s Membrane Permeability: A Computational Model Validated With in Vitro Permeability Assay Data

The journal of physical chemistry. B, 2017-05, Vol.121 (20), p.5228-5237

2017

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Effective methylation of phosphonic acids related to chemical warfare agents mediated by trimethyloxonium tetrafluoroborate for their qualitative detection and identification by gas chromatography-mass spectrometry

Analytica chimica acta, 2016-08, Vol.933 (C), p.134-143

2016

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Methylation protocol for the retrospective detection of isopropyl-, pinacolyl- and cyclohexylmethylphosphonic acids, indicative markers for the nerve agents sarin, soman and cyclosarin, at low levels in soils using EI-GC–MS

The Science of the total environment, 2019-09, Vol.683 (C), p.175-184

2019

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Comparison and analysis of zinc and cobalt-based systems as catalytic entities for the hydration of carbon dioxide

PloS one, 2013-06, Vol.8 (6), p.e66187-e66187

2013

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Carbene-based Difluoromethylation of Bisphenols: Application to the Instantaneous Tagging of Bisphenol A in Spiked Soil for Its Detection and Identification by Electron Ionization Gas Chromatography-Mass Spectrometry

Scientific reports, 2019-11, Vol.9 (1), p.17360-10, Article 17360

2019

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Use of carbonyldiimidazole as a derivatization agent for the detection of pinacolyl alcohol, a forensic marker for Soman, by EI‐GC–MS and LC‐HRMS in official OPCW proficiency test matrices

Journal of forensic sciences, 2024-07, Vol.69 (4), p.1256-1267

2024

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Unsaturated Sulfur Crown Ethers Can Extract Mercury(II) and Show Promise for Future Copernicium(II) Studies: A Combined Experimental and Computational Study

Inorganic chemistry, 2022-01, Vol.61 (2), p.807-817

2022

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Encapsulated liquid sorbents for carbon dioxide capture

Nature communications, 2015-02, Vol.6 (1), p.6124-6124, Article 6124

2015

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Detection and confirmation of fentanyls in high clay-content soil by electron ionization gas chromatography-mass spectrometry

Journal of forensic sciences, 2023-11, Vol.68 (6), p.2138-2152

2023

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Mechanically robust 3D graphene macroassembly with high surface area

Chemical communications (Cambridge, England), 2012-08, Vol.48 (67), p.8428-8430

2012

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Countermeasures for Preventing and Treating Opioid Overdose

Clinical pharmacology and therapeutics, 2021-03, Vol.109 (3), p.578-590

2021

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Trocylation of 3‐quinuclidinol, a key marker for the chemical warfare agent 3‐quinuclidinyl benzilate, for its enhanced detection at low levels in complex soil matrices by electron ionization gas chromatography–mass spectrometry

Rapid communications in mass spectrometry, 2021-08, Vol.35 (15), p.e9123-n/a

2021

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Analysis of Organophosphorus-Based Nerve Agent Degradation Products by Gas Chromatography-Mass Spectrometry (GC-MS): Current Derivatization Reactions in the Analytical Chemist’s Toolbox

Practical benzylation of N,N-substituted ethanolamines related to chemical warfare agents for analysis and detection by electron ionization gas chromatography-mass spectrometry

Trimethyloxonium-mediated methylation strategies for the rapid and simultaneous analysis of chlorinated phenols in various soils by electron impact gas chromatography-mass spectrometry

Analysis, identification and confirmation of synthetic opioids using chloroformate chemistry: Retrospective detection of fentanyl and acetylfentanyl in urine and plasma samples by EI-GC-MS and HR-LC-MS

Benzyl trichloroacetimidates as derivatizing agents for phosphonic acids related to nerve agents by EI-GC-MS during OPCW proficiency test scenarios

An efficient, optimized synthesis of fentanyl and related analogs

Evaluation of polyanionic cyclodextrins as high affinity binding scaffolds for fentanyl

Evaluation of 6-OxP-CD, an Oxime-based cyclodextrin as a viable medical countermeasure against nerve agent poisoning: Experimental and molecular dynamic simulation studies on its inclusion complexes with cyclosarin, soman and VX

Analysis of chemical warfare agents by gas chromatography-mass spectrometry: methods for their direct detection and derivatization approaches for the analysis of their degradation products

Structural modification of fentanyls for their retrospective identification by gas chromatographic analysis using chloroformate chemistry

Gas Chromatography-Mass Spectrometry Analysis of Synthetic Opioids Belonging to the Fentanyl Class: A Review

Development of a CNS-permeable reactivator for nerve agent exposure: an iterative, multi-disciplinary approach

Dose-dependent consequences of sub-chronic fentanyl exposure on neuron and glial co-cultures

Predicting a Drug’s Membrane Permeability: A Computational Model Validated With in Vitro Permeability Assay Data

Effective methylation of phosphonic acids related to chemical warfare agents mediated by trimethyloxonium tetrafluoroborate for their qualitative detection and identification by gas chromatography-mass spectrometry

Methylation protocol for the retrospective detection of isopropyl-, pinacolyl- and cyclohexylmethylphosphonic acids, indicative markers for the nerve agents sarin, soman and cyclosarin, at low levels in soils using EI-GC–MS

Comparison and analysis of zinc and cobalt-based systems as catalytic entities for the hydration of carbon dioxide

Carbene-based Difluoromethylation of Bisphenols: Application to the Instantaneous Tagging of Bisphenol A in Spiked Soil for Its Detection and Identification by Electron Ionization Gas Chromatography-Mass Spectrometry

Use of carbonyldiimidazole as a derivatization agent for the detection of pinacolyl alcohol, a forensic marker for Soman, by EI‐GC–MS and LC‐HRMS in official OPCW proficiency test matrices

Unsaturated Sulfur Crown Ethers Can Extract Mercury(II) and Show Promise for Future Copernicium(II) Studies: A Combined Experimental and Computational Study

Encapsulated liquid sorbents for carbon dioxide capture

Detection and confirmation of fentanyls in high clay-content soil by electron ionization gas chromatography-mass spectrometry

Mechanically robust 3D graphene macroassembly with high surface area

Countermeasures for Preventing and Treating Opioid Overdose

Trocylation of 3‐quinuclidinol, a key marker for the chemical warfare agent 3‐quinuclidinyl benzilate, for its enhanced detection at low levels in complex soil matrices by electron ionization gas chromatography–mass spectrometry

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