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The new engineering technique for the experimental investigation of physical and mechanical characteristics of thermal protective intumescent coatings is offered. A mathematical model is proposed for predicting the thermal behavior of structures protected by coatings; the model is closed by the studied material characteristics. The heating of a metal plate under standard thermal loading conditions is modeled mathematically. The modeling results are in good agreement with bench test results for metal temperature under the coating. The proposed technique of studying physical and mechanical characteristics can be applied to identify and monitor the state of thermal protective intumescent coatings in the long-term operation.