Details

Autor(en) / Beteiligte

• Villacís-Chiriboga, José
• Jacobs, Griet
• Van Camp, John
• Elst, Kathy
• Ruales, Jenny
• Marcillo-Parra, Verónica
• Böhm, Volker
• Bunea, Andrea
• Cirlini, Martina
• Craft, Neal
• De Meulenaer, Bruno
• Dias, M. Graça
• Lazzarino, Giacomo
• Meléndez-Martínez, Antonio J.
• Versloot, Pieter
• Mercadante, Adriana Z.
• Olmedilla-Alonso, Begoña
• Ortiz-Ulloa, Johana
• Stinco, Carla M.
• Voorspoels, Stefan

Titel

Interlaboratory exercise for the analysis of carotenoids and related compounds in dried mango fruit (Mangifera indica L.)

Ist Teil von

• Journal of food composition and analysis, 2022-08, Vol.111, p.104616, Article 104616

Ort / Verlag

Elsevier Inc

Erscheinungsjahr

2022

Quelle

Alma/SFX Local Collection

Beschreibungen/Notizen

• An interlaboratory comparison was done for the analysis of carotenoids in freeze-dried mango. The study was performed from July to September 2018. Mango fruit was freeze-dried, homogenized, and packaged under vacuum conditions in portions of 6 g (test sample). Two test samples were sent to the participating laboratories for analysis. Laboratory results were rated using Z-scores in accordance with ISO 13528 and ISO 17043. The standard deviation for proficiency assessment (also called target standard deviation) was determined using a modified Horwitz function and varied between 10% and 25%, depending on the analyte. Out of 14 laboratories from 10 different countries, 9 laboratories (64%) obtained a satisfactory performance (Z ≤ 2) for the analysis of β-carotene. While for 7 laboratories that analyzed α-carotene, (9Z)-β-carotene, β-cryptoxanthin, and zeaxanthin, 4 laboratories (57%) obtained a satisfactory performance. However, only 2 laboratories out of 7 (29%) obtained a satisfactory performance for lutein. Based on the comparability of the analytical results, this study concludes that freeze-dried mango pulp can be used as a reference material for the analysis of α and β-carotene, (9Z)-β-carotene, β-cryptoxanthin, and zeaxanthin by applying different analytical procedures for their extraction and quantification. [Display omitted] •State-of-the-art analytical techniques applied to analysis of mango carotenoids.•Good results for α and β-carotene, (9Z)-β-carotene, β-cryptoxanthin, and zeaxanthin.•Quantification of lutein demands extra efforts.•A Certified Reference Material is proposed based on analytical results