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Critical practical aspects in the application of liquid chromatography–mass spectrometric studies for the characterization of impurities and degradation products

Journal of pharmaceutical and biomedical analysis, 2014-01, Vol.87, p.191-217

2014

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Drug-Excipient Compatibility Study Through a Novel Vial-in-Vial Experimental Setup: A Benchmark Study

AAPS PharmSciTech, 2023-05, Vol.24 (5), p.117-117, Article 117

2023

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A critical review on the use of modern sophisticated hyphenated tools in the characterization of impurities and degradation products

Journal of pharmaceutical and biomedical analysis, 2012-10, Vol.69, p.148-173

2012

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Identification and characterization of GSK-9089 metabolites through high resolution-mass spectrometry based in vitro and in vivo rat biological sample analysis

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 2024-08, Vol.1244, p.124242, Article 124242

2024

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Modified NAP test: A simple and Responsive Nitrosating Methodology for Risk Evaluation of NDSRIs

Journal of pharmaceutical sciences, 2023-05, Vol.112 (5), p.1333-1340

2023

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Amalgamation of stress degradation and metabolite profiling in rat urine and feces for characterization of oxidative metabolites of flibanserin using UHPLC-Q-TOF-MS/MS, H/D exchange and NMR technique

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 2020-02, Vol.1139, p.121993-121993, Article 121993

2020

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A critical assessment on stability behaviour of Vorinostat using LC-MS-QTOF with H/D exchange and NMR

Journal of pharmaceutical and biomedical analysis, 2023-11, Vol.236, p.115687-115687, Article 115687

2023

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Drug-Leachable Interaction Product Evaluation in Prefilled Syringe of Ganirelix Acetate Injection

Journal of pharmaceutical sciences, 2024-08, Vol.113 (8), p.2023-2027

2024

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A systematic UHPLC-Q-TOF-MS/MS based analytical approach for characterization of flibanserin metabolites and establishment of biotransformation pathway

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 2021-11, Vol.1185, p.123011-123011, Article 123011

2021

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Hyphenated liquid chromatography - diode array detection - charged aerosol detection - high resolution - multistage mass spectrometry with online hydrogen/deuterium exchange: One stop solution for pharmaceutical impurity profiling

Journal of Chromatography A, 2023-01, Vol.1689, p.463725, Article 463725

2023

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Cell-Engineered Recombinant α‑Synuclein: A Gage R&R Validated Protocol

Journal of proteome research, 2024-01, Vol.23 (1), p.16-24

2024

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A comprehensive study on the identification and characterization of degradation products of lipoglycopeptide Dalbavancin using LC and LC-HRMS/MS

Journal of peptide science, 2024-05, p.e3608-e3608

2024

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Synthetic pharmaceutical peptides characterization by chromatography principles and method development

Journal of separation science, 2022-07, Vol.45 (13), p.2200-2216

2022

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Cutting-edge strategies and critical advancements in characterization and quantification of metabolites concerning translational metabolomics

Drug metabolism reviews, 2022-10, Vol.54 (4), p.401-426

2022

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LC and LC-HRMS studies on stability behavior of molnupiravir an anti-COVID 19 drug

Journal of liquid chromatography & related technologies, 2021-10, Vol.44 (15-16), p.750-759

2021

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Extrinsic hyaluronic acid induction differentially modulates intracellular glutamine metabolism in breast cancer stem cells

International journal of biological macromolecules, 2022-10, Vol.218, p.679-689

2022

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A rapid discriminative hydrogen-deuterium exchange and LC-HRMS/MS strategy for primary and higher order structural mapping of therapeutic proteins: a case study using filgrastim

Analytical methods, 2023-03, Vol.15 (12), p.1527-1535

2023

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Reactivity of N terminal histidine of peptides towards excipients/impurity of excipients: A case study of liraglutide excipient compatibility study

Journal of pharmaceutical sciences, 2024-08

2024

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LC-HRMS studies on ruxolitinib degradation: a comprehensive approach during drug development

Analytical methods, 2022-01, Vol.14 (4), p.480-490

2022

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LC-MS/TOF, LC-MSn, on-line H/D exchange and LC-NMR studies on rosuvastatin degradation and in silico determination of toxicity of its degradation products: a comprehensive approach during drug development

Analytical and bioanalytical chemistry, 2013-04, Vol.405 (10), p.3215-3231

2013

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LC-Q/TOF-HRMS and NMR Based Structural Characterization of the Major Photodegradation Impurity of Difluprednate

Chromatographia, 2022-07, Vol.85 (7), p.605-615

2022

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Identification and characterization of degradation products of irbesartan using LC-MS/TOF, MSn, on-line H/D exchange and LC-NMR

Journal of pharmaceutical and biomedical analysis, 2010-04, Vol.51 (5), p.1037-1046

2010

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Strategies for characterizing sildenafil, vardenafil, tadalafil and their analogues in herbal dietary supplements, and detecting counterfeit products containing these drugs

TrAC, Trends in analytical chemistry (Regular ed.), 2009, Vol.28 (1), p.13-28

2009

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Identification and characterization of degradation products of irbesartan using LC-MS/TOF, MS(n), on-line H/D exchange and LC-NMR

Journal of pharmaceutical and biomedical analysis, 2010-04, Vol.51 (5), p.1037-1046

2010

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Cross-linking of poly (vinyl alcohol) films under acidic and thermal stress

European journal of pharmaceutical sciences, 2020-09, Vol.152, p.105429-105429, Article 105429

2020

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Critical practical aspects in the application of liquid chromatography–mass spectrometric studies for the characterization of impurities and degradation products

Drug-Excipient Compatibility Study Through a Novel Vial-in-Vial Experimental Setup: A Benchmark Study

A critical review on the use of modern sophisticated hyphenated tools in the characterization of impurities and degradation products

Identification and characterization of GSK-9089 metabolites through high resolution-mass spectrometry based in vitro and in vivo rat biological sample analysis

Modified NAP test: A simple and Responsive Nitrosating Methodology for Risk Evaluation of NDSRIs

Amalgamation of stress degradation and metabolite profiling in rat urine and feces for characterization of oxidative metabolites of flibanserin using UHPLC-Q-TOF-MS/MS, H/D exchange and NMR technique

A critical assessment on stability behaviour of Vorinostat using LC-MS-QTOF with H/D exchange and NMR

Drug-Leachable Interaction Product Evaluation in Prefilled Syringe of Ganirelix Acetate Injection

A systematic UHPLC-Q-TOF-MS/MS based analytical approach for characterization of flibanserin metabolites and establishment of biotransformation pathway

Hyphenated liquid chromatography - diode array detection - charged aerosol detection - high resolution - multistage mass spectrometry with online hydrogen/deuterium exchange: One stop solution for pharmaceutical impurity profiling

Cell-Engineered Recombinant α‑Synuclein: A Gage R&R Validated Protocol

A comprehensive study on the identification and characterization of degradation products of lipoglycopeptide Dalbavancin using LC and LC-HRMS/MS

Synthetic pharmaceutical peptides characterization by chromatography principles and method development

Cutting-edge strategies and critical advancements in characterization and quantification of metabolites concerning translational metabolomics

LC and LC-HRMS studies on stability behavior of molnupiravir an anti-COVID 19 drug

Extrinsic hyaluronic acid induction differentially modulates intracellular glutamine metabolism in breast cancer stem cells

A rapid discriminative hydrogen-deuterium exchange and LC-HRMS/MS strategy for primary and higher order structural mapping of therapeutic proteins: a case study using filgrastim

Reactivity of N terminal histidine of peptides towards excipients/impurity of excipients: A case study of liraglutide excipient compatibility study

LC-HRMS studies on ruxolitinib degradation: a comprehensive approach during drug development

LC-MS/TOF, LC-MSn, on-line H/D exchange and LC-NMR studies on rosuvastatin degradation and in silico determination of toxicity of its degradation products: a comprehensive approach during drug development

LC-Q/TOF-HRMS and NMR Based Structural Characterization of the Major Photodegradation Impurity of Difluprednate

Identification and characterization of degradation products of irbesartan using LC-MS/TOF, MSn, on-line H/D exchange and LC-NMR

Strategies for characterizing sildenafil, vardenafil, tadalafil and their analogues in herbal dietary supplements, and detecting counterfeit products containing these drugs

Identification and characterization of degradation products of irbesartan using LC-MS/TOF, MS(n), on-line H/D exchange and LC-NMR

Cross-linking of poly (vinyl alcohol) films under acidic and thermal stress

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