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Reduced Pressure Ice Fog Technique for Controlled Ice Nucleation during Freeze-Drying

AAPS PharmSciTech, 2009-12, Vol.10 (4), p.1406-1411, Article 1406

2009

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Role of Thermodynamic, Molecular, and Kinetic Factors in Crystallization from the Amorphous State

Journal of pharmaceutical sciences, 2008-04, Vol.97 (4), p.1329-1349

2008

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Lyophilized Drug Product Cake Appearance: What Is Acceptable?

Journal of pharmaceutical sciences, 2017-07, Vol.106 (7), p.1706-1721

2017

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Mechanisms of protein stabilization in the solid state

Journal of pharmaceutical sciences, 2009-09, Vol.98 (9), p.2886-2908

2009

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Solubility advantage of amorphous pharmaceuticals: I. A thermodynamic analysis

Journal of pharmaceutical sciences, 2010-03, Vol.99 (3), p.1254-1264

2010

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Freeze-Drying Process Development and Scale-Up: Scale-Up of Edge Vial Versus Center Vial Heat Transfer Coefficients, K v

Journal of pharmaceutical sciences, 2016-11, Vol.105 (11), p.3333-3343

2016

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Design of freeze-drying processes for pharmaceuticals: practical advice

Pharmaceutical research, 2004-02, Vol.21 (2), p.191-200

2004

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Solubility Advantage of Amorphous Pharmaceuticals: II. Application of Quantitative Thermodynamic Relationships for Prediction of Solubility Enhancement in Structurally Diverse Insoluble Pharmaceuticals

Pharmaceutical research, 2010-12, Vol.27 (12), p.2704-2714

2010

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Determination of End Point of Primary Drying in Freeze-Drying Process Control

AAPS PharmSciTech, 2010-03, Vol.11 (1), p.73-84

2010

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Modeling the Secondary Drying Stage of Freeze Drying: Development and Validation of an Excel-Based Model

Journal of pharmaceutical sciences, 2017-03, Vol.106 (3), p.779-791

2017

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Emerging Freeze-Drying Process Development and Scale-up Issues

AAPS PharmSciTech, 2011-03, Vol.12 (1), p.372-378

2011

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The role of electroosmotic flow in transdermal iontophoresis

Advanced drug delivery reviews, 2001-03, Vol.46 (1), p.281-305

Pikal, Michael J.

2001

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Protein Stability During Freezing: Separation of Stresses and Mechanisms of Protein Stabilization

Pharmaceutical development and technology, 2007-01, Vol.12 (5), p.505-523

2007

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Calorimetric Investigation of the Structural Relaxation of Amorphous Materials: Evaluating Validity of the Methodologies

Journal of pharmaceutical sciences, 2005-05, Vol.94 (5), p.948-965

2005

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Mechanism of protein stabilization by sugars during freeze-drying and storage: Native structure preservation, specific interaction, and/or immobilization in a glassy matrix?

Journal of pharmaceutical sciences, 2005-07, Vol.94 (7), p.1427-1444

2005

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The Challenge of Drying Method Selection for Protein Pharmaceuticals: Product Quality Implications

Journal of pharmaceutical sciences, 2007-08, Vol.96 (8), p.1886-1916

2007

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Study of the Individual Contributions of Ice Formation and Freeze-Concentration on Isothermal Stability of Lactate Dehydrogenase during Freezing

Journal of pharmaceutical sciences, 2008-02, Vol.97 (2), p.798-814

2008

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Stabilization of proteins in solid form

Advanced drug delivery reviews, 2015-10, Vol.93, p.14-24

2015

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Role of Mechanical Stress in Crystallization and Relaxation Behavior of Amorphous Indomethacin

Journal of pharmaceutical sciences, 2008-10, Vol.97 (10), p.4446-4458

2008

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Heat and mass transfer scale-up issues during freeze drying: II. Control and characterization of the degree of supercooling

AAPS PharmSciTech, 2004-12, Vol.5 (4), p.e58-62

2004

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Use of manometric temperature measurement (MTM) and SMART™ freeze dryer technology for development of an optimized freeze‐drying cycle

Journal of pharmaceutical sciences, 2007-12, Vol.96 (12), p.3402-3418

2007

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Effect of sorbitol and residual moisture on the stability of lyophilized antibodies: Implications for the mechanism of protein stabilization in the solid state

Journal of pharmaceutical sciences, 2005-07, Vol.94 (7), p.1445-1455

2005

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Prediction of Onset of Crystallization from Experimental Relaxation Times. II. Comparison between Predicted and Experimental Onset Times

Journal of pharmaceutical sciences, 2008-01, Vol.97 (1), p.455-472

2008

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The Effect of Dryer Load on Freeze Drying Process Design

Journal of pharmaceutical sciences, 2010-10, Vol.99 (10), p.4363-4379

2010

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Stability of Freeze-Dried Protein Formulations: Contributions of Ice Nucleation Temperature and Residence Time in the Freeze-Concentrate

Journal of pharmaceutical sciences, 2020-06, Vol.109 (6), p.1896-1904

2020

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Reduced Pressure Ice Fog Technique for Controlled Ice Nucleation during Freeze-Drying

Role of Thermodynamic, Molecular, and Kinetic Factors in Crystallization from the Amorphous State

Lyophilized Drug Product Cake Appearance: What Is Acceptable?

Mechanisms of protein stabilization in the solid state

Solubility advantage of amorphous pharmaceuticals: I. A thermodynamic analysis

Freeze-Drying Process Development and Scale-Up: Scale-Up of Edge Vial Versus Center Vial Heat Transfer Coefficients, K v

Design of freeze-drying processes for pharmaceuticals: practical advice

Solubility Advantage of Amorphous Pharmaceuticals: II. Application of Quantitative Thermodynamic Relationships for Prediction of Solubility Enhancement in Structurally Diverse Insoluble Pharmaceuticals

Determination of End Point of Primary Drying in Freeze-Drying Process Control

Modeling the Secondary Drying Stage of Freeze Drying: Development and Validation of an Excel-Based Model

Emerging Freeze-Drying Process Development and Scale-up Issues

The role of electroosmotic flow in transdermal iontophoresis

Protein Stability During Freezing: Separation of Stresses and Mechanisms of Protein Stabilization

Calorimetric Investigation of the Structural Relaxation of Amorphous Materials: Evaluating Validity of the Methodologies

Mechanism of protein stabilization by sugars during freeze-drying and storage: Native structure preservation, specific interaction, and/or immobilization in a glassy matrix?

The Challenge of Drying Method Selection for Protein Pharmaceuticals: Product Quality Implications

Study of the Individual Contributions of Ice Formation and Freeze-Concentration on Isothermal Stability of Lactate Dehydrogenase during Freezing

Stabilization of proteins in solid form

Role of Mechanical Stress in Crystallization and Relaxation Behavior of Amorphous Indomethacin

Heat and mass transfer scale-up issues during freeze drying: II. Control and characterization of the degree of supercooling

Use of manometric temperature measurement (MTM) and SMART™ freeze dryer technology for development of an optimized freeze‐drying cycle

Effect of sorbitol and residual moisture on the stability of lyophilized antibodies: Implications for the mechanism of protein stabilization in the solid state

Prediction of Onset of Crystallization from Experimental Relaxation Times. II. Comparison between Predicted and Experimental Onset Times

The Effect of Dryer Load on Freeze Drying Process Design

Stability of Freeze-Dried Protein Formulations: Contributions of Ice Nucleation Temperature and Residence Time in the Freeze-Concentrate

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