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Optimization of pharmaceutical reactions using the dynamic response surface methodology

Computers & chemical engineering, 2020-04, Vol.135, p.106778, Article 106778

2020

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Constrained Version of the Dynamic Response Surface Methodology for Modeling Pharmaceutical Reactions

Industrial & engineering chemistry research, 2019-07, Vol.58 (30), p.13611-13621

2019

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Process Development and Scale Up of a Selective JAK3 Covalent Inhibitor PF-06651600

Organic process research & development, 2019-09, Vol.23 (9), p.1872-1880

2019

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Mild and Efficient DBU-Catalyzed Amidation of Cyanoacetates

Organic letters, 2009-05, Vol.11 (9), p.2003-2006

2009

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Toward the Identification of Stoichiometric Models for Complex Reaction Mixtures

Industrial & engineering chemistry research, 2023-02, Vol.62 (5), p.2225-2239

2023

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Machine learning directed multi-objective optimization of mixed variable chemical systems

Chemical engineering journal (Lausanne, Switzerland : 1996), 2023-01, Vol.451, p.138443, Article 138443

2023

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Stereoelectronic Effects in Ligand Design: Enantioselective Rhodium‐Catalyzed Hydrogenation of Aliphatic Cyclic Tetrasubstituted Enamides and Concise Synthesis of (R)‐Tofacitinib

Angewandte Chemie International Edition, 2019-09, Vol.58 (38), p.13573-13583

International ed. in English, 2019

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New Time Sampling Strategy for the Estimation of the Parameters in DRSM Models

Industrial & engineering chemistry research, 2020-07, Vol.59 (28), p.12792-12800

2020

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Kinetic and Data-Driven Reaction Analysis for Pharmaceutical Process Development

Industrial & engineering chemistry research, 2020-02, Vol.59 (6), p.2409-2421

2020

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Kinetic Parameter Estimation from Spectroscopic Data for a Multi-Stage Solid–Liquid Pharmaceutical Process

Organic process research & development, 2021-03, Vol.25 (3), p.373-383

2021

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Chemoselective Saponification in the Synthesis of Danuglipron Facilitated with Trifluoroethanol

Organic process research & development, 2024-07, Vol.28 (7), p.2702-2707

2024

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From dynamic response surface models to the identification of the reaction stoichiometry in a complex pharmaceutical case study

AIChE journal, 2019-04, Vol.65 (4), p.1173-1185

2019

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Probing the chemical ‘reactome’ with high-throughput experimentation data

Nature chemistry, 2024-04, Vol.16 (4), p.633-643

2024

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Developing a Multistep Continuous Manufacturing Process for (1R,2R)‑2-Amino-1-methylcyclopentan-1-ol

Organic process research & development, 2020-11, Vol.24 (11), p.2734-2744

2020

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Development of a Scalable Process for CI-1034, an Endothelin Antagonist

Organic process research & development, 2004-03, Vol.8 (2), p.201-212

2004

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Stoichiometry identification of pharmaceutical reactions using the constrained dynamic response surface methodology

AIChE journal, 2019-11, Vol.65 (11), p.n/a

2019

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Kinetic Modeling of API Oxidation: (2) Imipramine Stress Testing

Molecular pharmaceutics, 2022-05, Vol.19 (5), p.1526-1539

2022

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Kinetic Modeling of API Oxidation: (1) The AIBN/H2O/CH3OH Radical “Soup”

Molecular pharmaceutics, 2021-08, Vol.18 (8), p.3037-3049

2021

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Applications of Quantum Chemistry in Pharmaceutical Process Development: Current State and Opportunities

Organic process research & development, 2020-08, Vol.24 (8), p.1496-1507

2020

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Synthesis of Nirmatrelvir: Development of a Scalable Cobalt-Catalyzed Cyclopropanation for Manufacture of the Bicyclic [3.1.0]Proline-Building Block

Organic process research & development, 2023-12, Vol.27 (12), p.2260-2270

2023

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API Quality by Design Example from the Torcetrapib Manufacturing Process

Journal of pharmaceutical innovation, 2007-12, Vol.2 (3-4), p.71-86

2007

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Synthesis of Nirmatrelvir: Development of an Efficient, Scalable Process to Generate the Western Fragment

Organic process research & development, 2023-12, Vol.27 (12), p.2240-2249

2023

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Continuous Production of Anhydrous tert-Butyl Hydroperoxide in Nonane Using Membrane Pervaporation and Its Application in Flow Oxidation of a γ‑Butyrolactam

Organic process research & development, 2018-06, Vol.22 (6), p.707-720

2018

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Kinetic Modeling of API Oxidation: (1) The AIBN/H 2 O/CH 3 OH Radical "Soup"

Molecular pharmaceutics, 2021-08, Vol.18 (8), p.3037-3049

2021

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Commercial Route Research and Development for SGLT2 Inhibitor Candidate Ertugliflozin

Organic process research & development, 2014-01, Vol.18 (1), p.66-81

2014

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Optimization of pharmaceutical reactions using the dynamic response surface methodology

Constrained Version of the Dynamic Response Surface Methodology for Modeling Pharmaceutical Reactions

Process Development and Scale Up of a Selective JAK3 Covalent Inhibitor PF-06651600

Mild and Efficient DBU-Catalyzed Amidation of Cyanoacetates

Toward the Identification of Stoichiometric Models for Complex Reaction Mixtures

Machine learning directed multi-objective optimization of mixed variable chemical systems

Stereoelectronic Effects in Ligand Design: Enantioselective Rhodium‐Catalyzed Hydrogenation of Aliphatic Cyclic Tetrasubstituted Enamides and Concise Synthesis of (R)‐Tofacitinib

New Time Sampling Strategy for the Estimation of the Parameters in DRSM Models

Kinetic and Data-Driven Reaction Analysis for Pharmaceutical Process Development

Kinetic Parameter Estimation from Spectroscopic Data for a Multi-Stage Solid–Liquid Pharmaceutical Process

Chemoselective Saponification in the Synthesis of Danuglipron Facilitated with Trifluoroethanol

From dynamic response surface models to the identification of the reaction stoichiometry in a complex pharmaceutical case study

Probing the chemical ‘reactome’ with high-throughput experimentation data

Developing a Multistep Continuous Manufacturing Process for (1R,2R)‑2-Amino-1-methylcyclopentan-1-ol

Development of a Scalable Process for CI-1034, an Endothelin Antagonist

Stoichiometry identification of pharmaceutical reactions using the constrained dynamic response surface methodology

Kinetic Modeling of API Oxidation: (2) Imipramine Stress Testing

Kinetic Modeling of API Oxidation: (1) The AIBN/H2O/CH3OH Radical “Soup”

Applications of Quantum Chemistry in Pharmaceutical Process Development: Current State and Opportunities

Synthesis of Nirmatrelvir: Development of a Scalable Cobalt-Catalyzed Cyclopropanation for Manufacture of the Bicyclic [3.1.0]Proline-Building Block

API Quality by Design Example from the Torcetrapib Manufacturing Process

Synthesis of Nirmatrelvir: Development of an Efficient, Scalable Process to Generate the Western Fragment

Continuous Production of Anhydrous tert-Butyl Hydroperoxide in Nonane Using Membrane Pervaporation and Its Application in Flow Oxidation of a γ‑Butyrolactam

Kinetic Modeling of API Oxidation: (1) The AIBN/H 2 O/CH 3 OH Radical "Soup"

Commercial Route Research and Development for SGLT2 Inhibitor Candidate Ertugliflozin

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