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The Emergence of Universal Chromatographic Methods in the Research and Development of New Drug Substances

Accounts of chemical research, 2019-07, Vol.52 (7), p.1990-2002

2019

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Chaotropic Effects in Sub/Supercritical Fluid Chromatography via Ammonium Hydroxide in Water-Rich Modifiers: Enabling Separation of Peptides and Highly Polar Pharmaceuticals at the Preparative Scale

Analytical chemistry (Washington), 2019-11, Vol.91 (21), p.13907-13915

2019

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Macrocyclic glycopeptide chiral selectors bonded to core-shell particles enables enantiopurity analysis of the entire verubecestat synthetic route

Journal of Chromatography A, 2018-03, Vol.1539, p.87-92

2018

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Evaluation of global conformational changes in peptides and proteins following purification by supercritical fluid chromatography

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 2019-03, Vol.1110-1111, p.94-100

2019

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Comprehensive online multicolumn two-dimensional liquid chromatography-diode array detection-mass spectrometry workflow as a framework for chromatographic screening and analysis of new drug substances

Analytical and bioanalytical chemistry, 2020-04, Vol.412 (11), p.2655-2663

2020

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Supercritical fluid chromatography-photodiode array detection-electrospray ionization mass spectrometry as a framework for impurity fate mapping in the development and manufacture of drug substances

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 2018-03, Vol.1080, p.42-49

2018

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Chromatographic Resolution of Closely Related Species in Pharmaceutical Chemistry: Dehalogenation Impurities and Mixtures of Halogen Isomers

Analytical chemistry (Washington), 2014-01, Vol.86 (1), p.805-813

2014

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Unusual reversal of enantioselectivity in the asymmetric autocatalysis of pyrimidyl alkanol triggered by chiral aromatic alkanols and amines

Organic & biomolecular chemistry, 2017, Vol.15 (3), p.555-558

2017

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Can the analyte-triggered asymmetric autocatalytic Soai reaction serve as a universal analytical tool for measuring enantiopurity and assigning absolute configuration?

Organic & biomolecular chemistry, 2017, Vol.15 (1), p.96-11

2017

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Long-term development of the global energy sector under the influence of energy policies and technological progress

Russian journal of economics (Moskva), 2020-12, Vol.6 (4), p.347-357

2020

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Ultrafast Chiral Chromatography as the Second Dimension in Two-Dimensional Liquid Chromatography Experiments

Analytical chemistry (Washington), 2017-03, Vol.89 (6), p.3545-3553

2017

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Strategy for improving circular dichroism spectra deconvolution accuracy for macrocyclic peptides in drug discovery

Journal of pharmaceutical and biomedical analysis, 2025-01, Vol.252, p.116476, Article 116476

2025

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Combining size-exclusion chromatography with differential hydrogen–deuterium exchange to study protein conformational changes

Journal of Chromatography A, 2016-01, Vol.1431, p.224-230

2016

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Ultrafast chiral separations for high throughput enantiopurity analysis

Chemical communications (Cambridge, England), 2017, Vol.53 (3), p.509-512

2017

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Use of Raman spectroscopy and size-exclusion chromatography coupled with HDX-MS spectroscopy for studying conformational changes of small proteins in solution

Journal of pharmaceutical and biomedical analysis, 2020-09, Vol.189, p.113399-113399, Article 113399

2020

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New 1,3-Diynoic Derivatives of Natural Lembehyne B: Stereoselective Synthesis, Anticancer, and Neuritogenic Activity

ACS omega, 2020-02, Vol.5 (4), p.1974-1981

2020

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Interrogation of solution conformation of complex macrocyclic peptides utilizing a combined SEC-HDX-MS, circular dichroism, and NMR workflow

Analyst (London), 2022-01, Vol.147 (2), p.325-332

2022

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Solid-to-Liposome Conformational Transition of Phosphatidylcholine and Phosphatidylserine Probed by Atomic Force Microscopy, Infrared Spectroscopy, and Density Functional Theory Calculations

Analytical chemistry (Washington), 2022-09, Vol.94 (38), p.13243-13249

2022

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Enantioselective UHPLC Screening Combined with In Silico Modeling for Streamlined Development of Ultrafast Enantiopurity Assays

Analytical chemistry (Washington), 2022-01, Vol.94 (3), p.1804-1812

2022

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Use of MALDI-MS with solid-state hydrogen deuterium exchange for semi-automated assessment of peptide and protein physical stability in lyophilized solids

Analytica chimica acta, 2019-04, Vol.1054, p.114-121

2019

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High-throughput infrared spectroscopy for quantification of peptides in drug discovery

Journal of pharmaceutical and biomedical analysis, 2023-05, Vol.229, p.115350-115350, Article 115350

2023

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Rapid label-free cell-based Approach Membrane Permeability Assay using MALDI-hydrogen-deuterium exchange mass spectrometry for peptides

Analytica chimica acta, 2022-09, Vol.1225, p.340234-340234, Article 340234

2022

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Liposome Artificial Membrane Permeability Assay by MALDI-hydrogen-deuterium exchange mass spectrometry for peptides and small proteins

Analytica chimica acta, 2020-02, Vol.1099, p.111-118

2020

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Automated High-Throughput Matrix Assisted Laser Desorption Ionization Mass Spectrometry Methodology for Formulation Assessment of Polyethylene-Glycol-Conjugated Cytokine Proteins

Journal of pharmaceutical sciences, 2023-11, Vol.112 (11), p.2778-2782

2023

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Ultra-high-throughput SPE-MALDI workflow: Blueprint for efficient purification and screening of peptide libraries

Analytica chimica acta, 2021-01, Vol.1142, p.10-18

2021

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The Emergence of Universal Chromatographic Methods in the Research and Development of New Drug Substances

Chaotropic Effects in Sub/Supercritical Fluid Chromatography via Ammonium Hydroxide in Water-Rich Modifiers: Enabling Separation of Peptides and Highly Polar Pharmaceuticals at the Preparative Scale

Macrocyclic glycopeptide chiral selectors bonded to core-shell particles enables enantiopurity analysis of the entire verubecestat synthetic route

Evaluation of global conformational changes in peptides and proteins following purification by supercritical fluid chromatography

Comprehensive online multicolumn two-dimensional liquid chromatography-diode array detection-mass spectrometry workflow as a framework for chromatographic screening and analysis of new drug substances

Supercritical fluid chromatography-photodiode array detection-electrospray ionization mass spectrometry as a framework for impurity fate mapping in the development and manufacture of drug substances

Chromatographic Resolution of Closely Related Species in Pharmaceutical Chemistry: Dehalogenation Impurities and Mixtures of Halogen Isomers

Unusual reversal of enantioselectivity in the asymmetric autocatalysis of pyrimidyl alkanol triggered by chiral aromatic alkanols and amines

Can the analyte-triggered asymmetric autocatalytic Soai reaction serve as a universal analytical tool for measuring enantiopurity and assigning absolute configuration?

Long-term development of the global energy sector under the influence of energy policies and technological progress

Ultrafast Chiral Chromatography as the Second Dimension in Two-Dimensional Liquid Chromatography Experiments

Strategy for improving circular dichroism spectra deconvolution accuracy for macrocyclic peptides in drug discovery

Combining size-exclusion chromatography with differential hydrogen–deuterium exchange to study protein conformational changes

Ultrafast chiral separations for high throughput enantiopurity analysis

Use of Raman spectroscopy and size-exclusion chromatography coupled with HDX-MS spectroscopy for studying conformational changes of small proteins in solution

New 1,3-Diynoic Derivatives of Natural Lembehyne B: Stereoselective Synthesis, Anticancer, and Neuritogenic Activity

Interrogation of solution conformation of complex macrocyclic peptides utilizing a combined SEC-HDX-MS, circular dichroism, and NMR workflow

Solid-to-Liposome Conformational Transition of Phosphatidylcholine and Phosphatidylserine Probed by Atomic Force Microscopy, Infrared Spectroscopy, and Density Functional Theory Calculations

Enantioselective UHPLC Screening Combined with In Silico Modeling for Streamlined Development of Ultrafast Enantiopurity Assays

Use of MALDI-MS with solid-state hydrogen deuterium exchange for semi-automated assessment of peptide and protein physical stability in lyophilized solids

High-throughput infrared spectroscopy for quantification of peptides in drug discovery

Rapid label-free cell-based Approach Membrane Permeability Assay using MALDI-hydrogen-deuterium exchange mass spectrometry for peptides

Liposome Artificial Membrane Permeability Assay by MALDI-hydrogen-deuterium exchange mass spectrometry for peptides and small proteins

Automated High-Throughput Matrix Assisted Laser Desorption Ionization Mass Spectrometry Methodology for Formulation Assessment of Polyethylene-Glycol-Conjugated Cytokine Proteins

Ultra-high-throughput SPE-MALDI workflow: Blueprint for efficient purification and screening of peptide libraries

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