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Development of an Enantioselective [3 + 2] Cycloaddition To Synthesize the Pyrrolidine Core of ABBV-3221 on Multikilogram Scale

Organic process research & development, 2019-11, Vol.23 (11), p.2532-2537

2019

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Synthesis of 3,4,5-Trisubstituted Isoxazoles via Sequential [3 + 2] Cycloaddition/Silicon-Based Cross-Coupling Reactions

Journal of organic chemistry, 2005-04, Vol.70 (7), p.2839-2842

2005

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Palladium-Catalyzed Silylation of Aryl Bromides Leading to Functionalized Aryldimethylsilanols

Organic letters, 2003-09, Vol.5 (19), p.3483-3486

2003

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Development of the Enabling Route for Glecaprevir via Ring-Closing Metathesis

Organic process research & development, 2020-02, Vol.24 (2), p.183-200

2020

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Stereospecific Palladium-Catalyzed Cross-Coupling of (E)- and (Z)-Alkenylsilanolates with Aryl Chlorides

Journal of the American Chemical Society, 2006-12, Vol.128 (50), p.15958-15959

2006

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Development of a Large-Scale Route to Glecaprevir: Synthesis of the Macrocycle via Intramolecular Etherification

Organic process research & development, 2020-08, Vol.24 (8), p.1373-1392

2020

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A Kinetics-Based Approach for the Assignment of Reactivity Purge Factors

Organic process research & development, 2015-11, Vol.19 (11), p.1517-1523

2015

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New Semi-Automated Computer-Based System for Assessing the Purge of Mutagenic Impurities

Organic process research & development, 2019-11, Vol.23 (11), p.2470-2481

2019

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A consortium-driven framework to guide the implementation of ICH M7 Option 4 control strategies

Regulatory toxicology and pharmacology, 2017-11, Vol.90, p.22-28

2017

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Scalable Synthesis of a Cis-Substituted Cyclobutyl-Benzothiazole Pyridazinone: Process Development of an Efficient Copper Catalyzed C–N Cross-Coupling Reaction

Organic process research & development, 2014-01, Vol.18 (1), p.191-197

2014

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The Development of Continuous Process for Alkene Ozonolysis Based on Combined in Situ FTIR, Calorimetry, and Computational Chemistry

Organic process research & development, 2011-01, Vol.15 (1), p.91-97

2011

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Asymmetric Synthesis of Di- and Trisubstituted Cyclopropanes through an Intramolecular Ring Closure

Synlett, 2011-03, Vol.2011 (4), p.535-538

2011

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Improved Synthesis of 3-Substituted-4-amino-[3,2-c]-thienopyridines

Journal of organic chemistry, 2009-05, Vol.74 (10), p.3849-3855

2009

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Photochemical Synthesis of 3-Alkynals from 1-Alkynoxy-9,10-anthraquinones

Journal of organic chemistry, 2009-05, Vol.74 (10), p.3933-3935

2009

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Development of a Telescoped Alkylation/Reduction Reaction Sequence and an Asymmetric Hydrogenation to Enable the Kilogram Synthesis of ABBV-3748

Organic process research & development, 2022-10, Vol.26 (10), p.2947-2956

2022

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Continuous Process to Safely Manufacture an Aryldiazoacetate and Its Direct Use in a Dirhodium-Catalyzed Enantioselective Cyclopropanation

Organic process research & development, 2023-01, Vol.27 (1), p.90-104

2023

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Establishing Best Practice for the Application and Support of Solubility Purge Factors

Organic process research & development, 2023-10, Vol.27 (10), p.1751-1758

2023

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Enhanced Approaches to the Identification, Evaluation, and Control of Impurities

Journal of pharmaceutical innovation, 2019-06, Vol.14 (2), p.176-184

2019

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Photochemical Synthesis of Aldehydes in the Solid Phase

Journal of organic chemistry, 2002-04, Vol.67 (8), p.2677-2681

2002

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Author Correction: Enhanced Approaches to the Identification, Evaluation, and Control of Impurities

Journal of pharmaceutical innovation, 2019-06, Vol.14 (2), p.185-185

2019

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The Delivery of Flexibility from the Application of QbD to API Development

Journal of pharmaceutical innovation, 2018-12, Vol.13 (4), p.367-372

2018

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Studies on the silanol-based cross-coupling reaction: (1) Development of methods for the synthesis of aryl and heteroaryldimethysilanols, (2) Expansion of the substrate scope of the cross-coupling reaction and (3) Investigations on the transmetalation of organosilanols to transition metals

Kallemeyn, Jeffrey M

2007

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Studies on the silanol-based cross-coupling reaction: (1) Development of methods for the synthesis of aryl and heteroaryldimethysilanols, (2) Expansion of the substrate scope of the cross-coupling reaction and (3) Investigations on the transmetalation of organosilanols to transition metals

Kallemeyn, Jeffrey M

2007

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SYNTHESIS OF 3-PYRIDYLBORONIC ACID AND ITS PINACOL ESTER. APPLICATION OF 3-PYRIDYLBORONIC ACID IN SUZUKI COUPLING TO PREPARE 3-PYRIDIN-3-YLQUINOLINE

Organic syntheses, 2005, Vol.81, p.89

2005

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Stereospecific Palladium-Catalyzed Cross-Coupling of (E)- and (Z)-Alkenylsilanolates with Aryl Chlorides

ChemInform, 2007-04, Vol.38 (17), p.no-no

2007

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Development of an Enantioselective [3 + 2] Cycloaddition To Synthesize the Pyrrolidine Core of ABBV-3221 on Multikilogram Scale

Synthesis of 3,4,5-Trisubstituted Isoxazoles via Sequential [3 + 2] Cycloaddition/Silicon-Based Cross-Coupling Reactions

Palladium-Catalyzed Silylation of Aryl Bromides Leading to Functionalized Aryldimethylsilanols

Development of the Enabling Route for Glecaprevir via Ring-Closing Metathesis

Stereospecific Palladium-Catalyzed Cross-Coupling of (E)- and (Z)-Alkenylsilanolates with Aryl Chlorides

Development of a Large-Scale Route to Glecaprevir: Synthesis of the Macrocycle via Intramolecular Etherification

A Kinetics-Based Approach for the Assignment of Reactivity Purge Factors

New Semi-Automated Computer-Based System for Assessing the Purge of Mutagenic Impurities

A consortium-driven framework to guide the implementation of ICH M7 Option 4 control strategies

Scalable Synthesis of a Cis-Substituted Cyclobutyl-Benzothiazole Pyridazinone: Process Development of an Efficient Copper Catalyzed C–N Cross-Coupling Reaction

The Development of Continuous Process for Alkene Ozonolysis Based on Combined in Situ FTIR, Calorimetry, and Computational Chemistry

Asymmetric Synthesis of Di- and Trisubstituted Cyclopropanes through an Intramolecular Ring Closure

Improved Synthesis of 3-Substituted-4-amino-[3,2-c]-thienopyridines

Photochemical Synthesis of 3-Alkynals from 1-Alkynoxy-9,10-anthraquinones

Development of a Telescoped Alkylation/Reduction Reaction Sequence and an Asymmetric Hydrogenation to Enable the Kilogram Synthesis of ABBV-3748

Continuous Process to Safely Manufacture an Aryldiazoacetate and Its Direct Use in a Dirhodium-Catalyzed Enantioselective Cyclopropanation

Establishing Best Practice for the Application and Support of Solubility Purge Factors

Enhanced Approaches to the Identification, Evaluation, and Control of Impurities

Photochemical Synthesis of Aldehydes in the Solid Phase

Author Correction: Enhanced Approaches to the Identification, Evaluation, and Control of Impurities

The Delivery of Flexibility from the Application of QbD to API Development

Studies on the silanol-based cross-coupling reaction: (1) Development of methods for the synthesis of aryl and heteroaryldimethysilanols, (2) Expansion of the substrate scope of the cross-coupling reaction and (3) Investigations on the transmetalation of organosilanols to transition metals

Studies on the silanol-based cross-coupling reaction: (1) Development of methods for the synthesis of aryl and heteroaryldimethysilanols, (2) Expansion of the substrate scope of the cross-coupling reaction and (3) Investigations on the transmetalation of organosilanols to transition metals

SYNTHESIS OF 3-PYRIDYLBORONIC ACID AND ITS PINACOL ESTER. APPLICATION OF 3-PYRIDYLBORONIC ACID IN SUZUKI COUPLING TO PREPARE 3-PYRIDIN-3-YLQUINOLINE

Stereospecific Palladium-Catalyzed Cross-Coupling of (E)- and (Z)-Alkenylsilanolates with Aryl Chlorides

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