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Perspectives on the Designation of Oligonucleotide Starting Materials

Nucleic acid therapeutics, 2021-04, Vol.31 (2), p.93-113

2021

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Development of Kilogram-Scale Convergent Liquid-Phase Synthesis of Oligonucleotides

Journal of organic chemistry, 2022-02, Vol.87 (4), p.2087-2110

2022

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The Chelate Effect Rationalizes Observed Rate Acceleration and Enantioselectivity in BINOL‐Catalyzed Petasis Reactions

Chemistry : a European journal, 2023-03, Vol.29 (13), p.e202203331-n/a

2023

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A1 adenosine receptor antagonists, agonists, and allosteric enhancers

Handbook of experimental pharmacology, 2009 (193), p.25

2009

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Solid-Phase Synthesis of Phosphorothioate Oligonucleotides Using Sulfurization Byproducts for in Situ Capping

Journal of organic chemistry, 2018-10, Vol.83 (19), p.11577-11585

2018

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Catalytic Asymmetric Petasis Reactions of Vinylboronates

Journal of organic chemistry, 2013-09, Vol.78 (18), p.9415-9423

2013

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Synthesis of Vixotrigine, a Voltage- and Use-Dependent Sodium Channel Blocker. Part 2: Development of a Late-Stage Process

Organic process research & development, 2020-12, Vol.24 (12), p.2814-2829

2020

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Acceleration of Petasis Reactions of Salicylaldehyde Derivatives with Molecular Sieves

Journal of organic chemistry, 2012-01, Vol.77 (2), p.1154-1160

2012

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Process Development of an N‑Benzylated Chloropurine at the Kilogram Scale

Organic process research & development, 2015-03, Vol.19 (3), p.437-443

2015

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Case Studies in the Applicability of Drug Substance Design Spaces Developed on the Laboratory Scale to Commercial Manufacturing

Organic process research & development, 2015-08, Vol.19 (8), p.925-934

2015

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Case Studies in the Development of Drug Substance Control Strategies

Organic process research & development, 2015-08, Vol.19 (8), p.935-948

2015

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Part 1: A Review and Perspective of the Regulatory Guidance to Support Designation and Justification of API Starting Material

Organic process research & development, 2014-05, Vol.18 (5), p.587-593

2014

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Part 2: Designation and Justification of API Starting Materials: Current Practices across Member Companies of the IQ Consortium

Organic process research & development, 2014-05, Vol.18 (5), p.594-600

2014

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Part 3: Designation and Justification of API Starting Materials: Proposed Framework for Alignment from an Industry Perspective

Organic process research & development, 2015-08, Vol.19 (8), p.915-924

2015

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Tricyclic Imidazoline Derivatives as Potent and Selective Adenosine A1 Receptor Antagonists

Journal of medicinal chemistry, 2006-11, Vol.49 (24), p.7132-7139

2006

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Understanding and Control of Dimethyl Sulfate in a Manufacturing Process: Kinetic Modeling of a Fischer Esterification Catalyzed by H2SO4

Organic process research & development, 2012-02, Vol.16 (2), p.232-239

2012

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Potent and Orally Bioavailable 8-Bicyclo[2.2.2]octylxanthines as Adenosine A1 Receptor Antagonists

Journal of medicinal chemistry, 2006-11, Vol.49 (24), p.7119-7131

2006

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Soluble Catalysts for Improved Pschorr Cyclizations

Journal of organic chemistry, 1995-01, Vol.60 (1), p.196-201

1995

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Detection of Aryl Radicals in Hydrodediazoniations

Journal of organic chemistry, 1997-11, Vol.62 (24), p.8304-8308

1997

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Highly Regio- and Enantioselective Catalytic Hydrogenation of Enamides in Conjugated Diene Systems: Synthesis and Application of γ,δ-Unsaturated Amino Acids

Journal of the American Chemical Society, 1998-02, Vol.120 (4), p.657-663

1998

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Synthesis of alkyne derivatives of a novel triazolopyrazine as A2A adenosine receptor antagonists

Bioorganic & medicinal chemistry letters, 2005-02, Vol.15 (3), p.511-515

2005

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Development of an Early Phase Process for a Potent Oligodendrocyte Precursor Cell Differentiator

Organic process research & development, 2024-06, Vol.28 (6), p.2203-2212

2024

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Norbornyllactone-substituted xanthines as adenosine A1 receptor antagonists

Bioorganic & medicinal chemistry, 2006-06, Vol.14 (11), p.3654-3661

2006

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Lewis-acid catalysis of the asymmetric Diels–Alder reaction of dimenthyl fumarate and cyclopentadiene

Tetrahedron: asymmetry, 2002-06, Vol.13 (9), p.957-960

2002

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Process Development and Large-Scale Synthesis of BTK Inhibitor BIIB068

Organic process research & development, 2020-06, Vol.24 (6), p.1199-1206

2020

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Perspectives on the Designation of Oligonucleotide Starting Materials

Development of Kilogram-Scale Convergent Liquid-Phase Synthesis of Oligonucleotides

The Chelate Effect Rationalizes Observed Rate Acceleration and Enantioselectivity in BINOL‐Catalyzed Petasis Reactions

A1 adenosine receptor antagonists, agonists, and allosteric enhancers

Solid-Phase Synthesis of Phosphorothioate Oligonucleotides Using Sulfurization Byproducts for in Situ Capping

Catalytic Asymmetric Petasis Reactions of Vinylboronates

Synthesis of Vixotrigine, a Voltage- and Use-Dependent Sodium Channel Blocker. Part 2: Development of a Late-Stage Process

Acceleration of Petasis Reactions of Salicylaldehyde Derivatives with Molecular Sieves

Process Development of an N‑Benzylated Chloropurine at the Kilogram Scale

Case Studies in the Applicability of Drug Substance Design Spaces Developed on the Laboratory Scale to Commercial Manufacturing

Case Studies in the Development of Drug Substance Control Strategies

Part 1: A Review and Perspective of the Regulatory Guidance to Support Designation and Justification of API Starting Material

Part 2: Designation and Justification of API Starting Materials: Current Practices across Member Companies of the IQ Consortium

Part 3: Designation and Justification of API Starting Materials: Proposed Framework for Alignment from an Industry Perspective

Tricyclic Imidazoline Derivatives as Potent and Selective Adenosine A1 Receptor Antagonists

Understanding and Control of Dimethyl Sulfate in a Manufacturing Process: Kinetic Modeling of a Fischer Esterification Catalyzed by H2SO4

Potent and Orally Bioavailable 8-Bicyclo[2.2.2]octylxanthines as Adenosine A1 Receptor Antagonists

Soluble Catalysts for Improved Pschorr Cyclizations

Detection of Aryl Radicals in Hydrodediazoniations

Highly Regio- and Enantioselective Catalytic Hydrogenation of Enamides in Conjugated Diene Systems: Synthesis and Application of γ,δ-Unsaturated Amino Acids

Synthesis of alkyne derivatives of a novel triazolopyrazine as A2A adenosine receptor antagonists

Development of an Early Phase Process for a Potent Oligodendrocyte Precursor Cell Differentiator

Norbornyllactone-substituted xanthines as adenosine A1 receptor antagonists

Lewis-acid catalysis of the asymmetric Diels–Alder reaction of dimenthyl fumarate and cyclopentadiene

Process Development and Large-Scale Synthesis of BTK Inhibitor BIIB068

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