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A Process in Need Is a Process Indeed: Scalable Enantioselective Synthesis of Chiral Compounds for the Pharmaceutical Industry

Chemistry : a European journal, 2003-01, Vol.9 (2), p.378-388

Ikunaka, Masaya

2003

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Synthesis of (S)-3-(N-Methylamino)-1-(2-thienyl)propan-1-ol: Revisiting Eli Lilly's Resolution−Racemization−Recycle Synthesis of Duloxetine for Its Robust Processes

Organic process research & development, 2006-09, Vol.10 (5), p.905-913

2006

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Synthetic Studies on Novel 1,4-Dihydro-2-methylthio-4,4,6-trisubstituted Pyrimidine-5-carboxylic Acid Esters and Their Tautomers

Chemical and Pharmaceutical Bulletin, 2011/12/01, Vol.59(12), pp.1458-1466

2011

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Catalytic Asymmetric Carbon−Carbon Bond Formations: Their Evolution from Biocatalysis to Organocatalysis over the Millennium

Organic process research & development, 2007-05, Vol.11 (3), p.495-502

Ikunaka, Masaya

2007

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PTC in OPRD: An Illustrative Overview

Organic process research & development, 2008-07, Vol.12 (4), p.698-709

Ikunaka, Masaya

2008

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Bacillus subtilis epoxide hydrolase-catalyzed preparation of enantiopure 2-methylpropane-1,2,3-triol monobenzyl ether and its application to expeditious synthesis of ( R)-bicalutamide

Tetrahedron letters, 2007-02, Vol.48 (6), p.979-983

2007

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A Practical RuCl3-Catalyzed Oxidation Using Trichloroisocyanuric Acid As a Stoichiometric Oxidant under Mild Nonacidic Conditions

Organic process research & development, 2004-11, Vol.8 (6), p.931-938

2004

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Synthetic Studies on Novel 1,4-Dihydro-2-methylthio-4,4,6-trisubstituted Pyrimidine-5-carboxylic Acid Esters and Their Tautomers

Chemical & Pharmaceutical Bulletin, 2011, Vol.59 (12), p.1458-1467

2011

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An Expeditious Scalable Synthesis of (S)-2-Amino-5-methoxytetralin via Resolution

Organic process research & development, 2005-01, Vol.9 (1), p.30-38

2005

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N,N-Diethyl-(R)-[3-(2-aminopropyl)-1H-indol-7-yloxy]acetamide: Its Process Chemistry Ranging from Enantiocontrolled Construction of the Chiral Amine Side Chain to Regioselective Functionalization of the Aromatic Starting Materials

Organic process research & development, 2007-01, Vol.11 (1), p.73-80

2007

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A concise synthesis of (2 S,3 S)-BocAHPBA and ( R)-BocDMTA, chiral building blocks for peptide-mimetic HIV protease inhibitors

Tetrahedron: asymmetry, 2002-06, Vol.13 (11), p.1201-1208

2002

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Biocatalysis from the perspective of an industrial practitioner: let a biocatalyst do a job that no chemocatalyst can

Catalysis today, 2004, Vol.96 (3), p.93-102

Ikunaka, Masaya

2004

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Microbial hydroxylation of indole to 7-hydroxyindole by Acinetobacter calcoaceticus strain 4-1-5

Bioscience, biotechnology, and biochemistry, 2004-05, Vol.68 (5), p.1167-1169

2004

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Stereoselective synthesis of a novel 2-aza-7-oxabicyclo[3.3.0]octane as neurokinin-1 receptor antagonist

Bioorganic & medicinal chemistry letters, 2007-12, Vol.17 (24), p.6887-6890

2007

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A practical chemoenzymatic process to access ( R)-quinuclidin-3-ol on scale

Tetrahedron: asymmetry, 2003-07, Vol.14 (13), p.1871-1877

2003

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A Scalable Synthesis of (R)-3,5-Dihydro-4H-dinaphth[2,1-c:1‘2‘-e]azepine

Organic process research & development, 2003-09, Vol.7 (5), p.644-648

2003

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A Practical RuCl 3 -Catalyzed Oxidation Using Trichloroisocyanuric Acid As a Stoichiometric Oxidant under Mild Nonacidic Conditions

Organic process research & development, 2004-11, Vol.8 (6), p.931-938

2004

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A scalable chemoenzymatic preparation of ( R)-tetrahydrofuran-2-carboxylic acid

Tetrahedron: asymmetry, 2003-05, Vol.14 (10), p.1385-1391

2003

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A practical enantioselective synthesis of ( S)-3-hydroxytetradecanoic acid

Tetrahedron: asymmetry, 1999-07, Vol.10 (15), p.2945-2950

1999

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An Enantioselective Synthesis of (2S,3R)-3-(N-Benzyloxycarbonyl)amino-1-chloro-4-phenylthiobutan-2-ol, a Central Intermediate of Nelfinavir1

Organic process research & development, 2002-01, Vol.6 (1), p.49-53

2002

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The Highly Selective Equatorial Hydride Delivery by Biocatalysis: Chemoenzymatic Synthesis of trans-2-(4-Propylcyclohexyl)-1,3-propanediol via cis-4-Propylcyclohexanol

Organic process research & development, 2004-05, Vol.8 (3), p.389-395

2004

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A Scalable Synthesis of ( R )-3,5-Dihydro-4 H -dinaphth[2,1- c :1‘2‘- e ]azepine

Organic process research & development, 2003-09, Vol.7 (5), p.644-648

2003

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ChemInform Abstract: PTC in OPRD: An Illustrative Overview

ChemInform, 2008-11, Vol.39 (46), p.no-no

Ikunaka, Masaya

2008

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A scalable synthesis of ( R)-3-(2-aminopropyl)-7-benzyloxyindole via resolution

Tetrahedron: asymmetry, 2001-12, Vol.12 (23), p.3235-3240

2001

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Synthesis of all of the four energetically possible stereoisomers of 7-ethyl-2-methyl-1,6-dioxaspiro[4.5]decane

Tetrahedron, 1984-01, Vol.40 (18), p.3471-3479

1984

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A Process in Need Is a Process Indeed: Scalable Enantioselective Synthesis of Chiral Compounds for the Pharmaceutical Industry

Synthesis of (S)-3-(N-Methylamino)-1-(2-thienyl)propan-1-ol: Revisiting Eli Lilly's Resolution−Racemization−Recycle Synthesis of Duloxetine for Its Robust Processes

Synthetic Studies on Novel 1,4-Dihydro-2-methylthio-4,4,6-trisubstituted Pyrimidine-5-carboxylic Acid Esters and Their Tautomers

Catalytic Asymmetric Carbon−Carbon Bond Formations: Their Evolution from Biocatalysis to Organocatalysis over the Millennium

PTC in OPRD: An Illustrative Overview

Bacillus subtilis epoxide hydrolase-catalyzed preparation of enantiopure 2-methylpropane-1,2,3-triol monobenzyl ether and its application to expeditious synthesis of ( R)-bicalutamide

A Practical RuCl3-Catalyzed Oxidation Using Trichloroisocyanuric Acid As a Stoichiometric Oxidant under Mild Nonacidic Conditions

Synthetic Studies on Novel 1,4-Dihydro-2-methylthio-4,4,6-trisubstituted Pyrimidine-5-carboxylic Acid Esters and Their Tautomers

An Expeditious Scalable Synthesis of (S)-2-Amino-5-methoxytetralin via Resolution

N,N-Diethyl-(R)-[3-(2-aminopropyl)-1H-indol-7-yloxy]acetamide: Its Process Chemistry Ranging from Enantiocontrolled Construction of the Chiral Amine Side Chain to Regioselective Functionalization of the Aromatic Starting Materials

A concise synthesis of (2 S,3 S)-BocAHPBA and ( R)-BocDMTA, chiral building blocks for peptide-mimetic HIV protease inhibitors

Biocatalysis from the perspective of an industrial practitioner: let a biocatalyst do a job that no chemocatalyst can

Microbial hydroxylation of indole to 7-hydroxyindole by Acinetobacter calcoaceticus strain 4-1-5

Stereoselective synthesis of a novel 2-aza-7-oxabicyclo[3.3.0]octane as neurokinin-1 receptor antagonist

A practical chemoenzymatic process to access ( R)-quinuclidin-3-ol on scale

A Scalable Synthesis of (R)-3,5-Dihydro-4H-dinaphth[2,1-c:1‘2‘-e]azepine

A Practical RuCl 3 -Catalyzed Oxidation Using Trichloroisocyanuric Acid As a Stoichiometric Oxidant under Mild Nonacidic Conditions

A scalable chemoenzymatic preparation of ( R)-tetrahydrofuran-2-carboxylic acid

A practical enantioselective synthesis of ( S)-3-hydroxytetradecanoic acid

An Enantioselective Synthesis of (2S,3R)-3-(N-Benzyloxycarbonyl)amino-1-chloro-4-phenylthiobutan-2-ol, a Central Intermediate of Nelfinavir1

The Highly Selective Equatorial Hydride Delivery by Biocatalysis: Chemoenzymatic Synthesis of trans-2-(4-Propylcyclohexyl)-1,3-propanediol via cis-4-Propylcyclohexanol

A Scalable Synthesis of ( R )-3,5-Dihydro-4 H -dinaphth[2,1- c :1‘2‘- e ]azepine

ChemInform Abstract: PTC in OPRD: An Illustrative Overview

A scalable synthesis of ( R)-3-(2-aminopropyl)-7-benzyloxyindole via resolution

Synthesis of all of the four energetically possible stereoisomers of 7-ethyl-2-methyl-1,6-dioxaspiro[4.5]decane

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