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Microporous and mesoporous materials, 2001-11, Vol.48 (1), p.31-37
Ort / Verlag
Amsterdam: Elsevier Inc
Erscheinungsjahr
2001
Quelle
Access via ScienceDirect (Elsevier)
Beschreibungen/Notizen
Zeolite beta was crystallized from clear homogeneous solutions within the pores of anion exchange resin beads. The organic macrotemplate was then removed by combustion leaving stable macrospheres of zeolite beta. The zeolite beta crystallization within the resin beads was investigated by X-ray diffraction, Raman spectroscopy, SEM and nitrogen adsorption measurements. Crystallization within the macrotemplates was compared with the crystallization from bulk solution. The influence of the resin beads on the crystallization process was investigated by increasing the amount of ion exchanger present during synthesis and also by preparing bulk samples in the absence of macrotemplates.