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Structural and magnetic features of the solid-state synthesis and martensitic transformations in Ni/Fe(0 0 1)/MgO(0 0 1) thin films
Ist Teil von
Journal of magnetism and magnetic materials, 2007-03, Vol.310 (1), p.126-130
Ort / Verlag
Amsterdam: Elsevier B.V
Erscheinungsjahr
2007
Link zum Volltext
Quelle
Elsevier ScienceDirect Journals Complete
Beschreibungen/Notizen
The results of the experimental study of phase transformations occurring in Ni/Fe(0
0
1)/MgO(0
0
1) thin films with 3Fe:1Ni atomic composition during annealing at temperatures up to 650
°C and cooling to liquid nitrogen temperature are presented. Comparative analysis of previous and current results suggests that the paramagnetic phase γ
par present in the invar of Ni
1−
x
Fe
x
alloys is the γ-Fe
3Ni phase with the lattice parameter
a=0.3600
nm. Measurements of magnetization of the samples in dependence of composition allowed one to determine a single-phase region of γ
par phase existence in thin films limited by 75
at% Fe. It is shown that the temperature of γ
par phase initiation during the solid-state synthesis coincides with the temperature
A
S of the reverse martensitic α′→γ
par transition (
A
S=
T
0∼550
°C).