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Dendritic morphologies of directionally solidified single crystals along different crystallographic orientations
Ist Teil von
Journal of crystal growth, 2002-03, Vol.236 (1), p.420-428
Ort / Verlag
Amsterdam: Elsevier B.V
Erscheinungsjahr
2002
Quelle
Elsevier Journal Backfiles on ScienceDirect (DFG Nationallizenzen)
Beschreibungen/Notizen
Pb-2.2
wt% Sb alloy was directionally solidified along [1
0
0], [1
1
0] and [1
1
1] crystallographic orientations using pure lead single crystal seeds, with a positive thermal gradient of 140
K
cm
−1 and growth rate of 10
μm
s
−1, and then quenched. Longitudinal (parallel to the growth direction) and transverse microstructures in the mushy region and in the quenched portion ahead of the solidification front were examined to investigate the morphology of primary dendrites solidified along different crystallographic orientations. Transverse microstructures showed that for growth along [1
0
0] the primary dendrites had the usual four-fold symmetry due to side-branching; for [1
1
0] orientation, they appeared plate like; while for [1
1
1] orientation, a uniform distribution of nodes was observed. These observations confirm that side-branches in FCC metal alloys grow along 〈1
0
0〉 crystallographic directions irrespective of heat-extraction direction.