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We have synthesized layered inclusion (intercalation) compounds with the general formula (C
2
F
x
Br
0.01
·
y
G)
n
, where (C
2
F
x
Br
0.01
)
n
is a host component, G stands for ethyl acetate (guest component), 0.5 <
x
< 1.0,
y
1
= 0.109–0.162 (stage 1), and
y
2
= 0.052–0.074 (stage 2). Using IR spectroscopy, we studied the behavior of the functional groups in the guest and host subsystems. The influence of the composition (structure) of the polymer host (C
2
F
x
Br
0.01
)
n
on the properties of the synthesized compounds was studied using physicochemical characterization techniques (differential thermal analysis and X-ray diffraction).