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Details

Autor(en) / Beteiligte
Titel
Synthesis of Si3N4-Based Powder Composites for Ceramic Fabrication by Spark Plasma Sintering
Ist Teil von
  • Inorganic materials, 2022-10, Vol.58 (10), p.1098-1104
Ort / Verlag
Moscow: Pleiades Publishing
Erscheinungsjahr
2022
Link zum Volltext
Quelle
Alma/SFX Local Collection
Beschreibungen/Notizen
  • — There were examined four ways of applying sintering additives (Y 2 O 3 : Al 2 O 3 = 3 : 5) to particles of commercial Si 3 N 4 powders differing in particle size composition: amorphous nanopowder and microcrystalline α-Si 3 N 4 powder. The oxide sintering additive coating was produced in two steps: wet chemical preparation of the starting Si 3 N 4 powder with compounds containing yttrium and aluminum ions and annealing of the resultant powder composites at a temperature of 1000°C in air. The way the sintering addition is applied and the particle size composition of the starting Si 3 N 4 powder have been shown to influence the composition of the crystalline phases forming during annealing. The optimal process for obtaining Si 3 N 4 ceramics with improved physical and mechanical properties is spray drying, which makes it possible to obtain spherical agglomerates.

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