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Standardization of an 55Fe solution using the TDCR method in POLATOM as part of the CCRI (II)-K2.Fe-55.2019 key comparison
Ist Teil von
Journal of radioanalytical and nuclear chemistry, 2022, Vol.331 (8), p.3241-3248
Ort / Verlag
Cham: Springer International Publishing
Erscheinungsjahr
2022
Quelle
Alma/SFX Local Collection
Beschreibungen/Notizen
Measurements were made using the TDCR method. POLATOM prepared and distributed for the key comparison participants the
55
Fe solution and
55
Fe ready-to-measure sources in the Ultima Gold™ scintillator in polyethylene vials. The stability of the sources was confirmed. Source counting efficiency decreased proportionally with time by about 0.7% per month, possibly due to colour quenching. The POLATOM measurement result was consistent with the key comparison reference value. The nuclear data for
55
Fe were adopted in accordance with the KCWG(II) recommendation. Measurement results obtained in non-diffusive (glass) vials were lower than in diffusive vials.