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Effect of microstructural evolution from nano to micron grain size regime towards structural, magnetic, electrical and microwave properties of gadolinium iron garnet (Gd3Fe5O12)
Ist Teil von
Journal of materials science. Materials in electronics, 2021-04, Vol.32 (8), p.10160-10179
Ort / Verlag
New York: Springer US
Erscheinungsjahr
2021
Quelle
Alma/SFX Local Collection
Beschreibungen/Notizen
The influence of microstructural changes from nano to micron grain size regime towards their structural, magnetic, electrical and microwave properties of gadolinium iron garnet (Gd
3
Fe
5
O
12
) has been investigated systematically in this research work. Raw materials were milled via high-energy ball milling (HEBM) followed by subsequent sintering (600–1400 °C) process. X-ray diffraction (XRD) analysis had shown that single phase with garnet structure and highest crystallinity of Gd
3
Fe
5
O
12
was formed at 1000 °C. The
B
–
H
hysteresis loop unveil the evolution development of magnetic behaviour (paramagnetism–ferrimagnetism) in samples thru variation of different sintering temperature. The values of linewidth (
∆H
) can be grouped into two groups which are; sample increased from 600 to 1000 °C due to shape and strain induced anisotropy while decreasing from 1100 to 1400 °C influenced by magnetocrystalline anisotropy with the increment of the sintering temperature.