Details

Autor(en) / Beteiligte

• Abdullah, Hayder B.
• Irmawati, Ramli
• Ismail, Ismayadi
• Yusof, Nor Azah

Titel

Direct synthesis of carbon nanotube aerogel using floating catalyst chemical vapor deposition: effect of gas flow rate

Ist Teil von

• Chemical papers, 2020-10, Vol.74 (10), p.3359-3365

Ort / Verlag

Cham: Springer International Publishing

Erscheinungsjahr

2020

Quelle

Alma/SFX Local Collection

Beschreibungen/Notizen

• Carbon nanotube aerogel (CNT aerogel) was synthesized through the catalytic decomposition of toluene in the mixture of ferrocene and thiophene through floating catalyst chemical vapor deposition method. This study described the effect of (Ar and H 2 ) carrier gas flow rate on the quality and yield of CNT aerogel. Results indicated that the flow rate of the gas was an important parameter which helped in determining the yield and quality of the CNTs. The CNTs are multiwalled with its diameter decreased when the H 2 flow rate was increased. Scanning electron microscopy indicated the average diameter of ≈ 31, 30, 27, 26, 18, and 15 nm when the H 2 flow rate was increased from 400, 450, 500, 550, 600, 650 sccm, respectively. Furthermore, elemental analysis with energy dispersion spectrum for CNT aerogel produced at 600 sccm resulted in a 96.22 wt% carbons along with 3.78 wt% iron in the CNT aerogel sample. Results indicated that a hydrogen flow rate of 600 sccm produced high yield and good CNTs morphology.