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Heat distribution in Paris-Edinburgh press assemblies through finite element simulations
Ist Teil von
High pressure research, 2018-07, Vol.38 (3), p.303-324
Ort / Verlag
Abingdon: Taylor & Francis
Erscheinungsjahr
2018
Quelle
Taylor & Francis
Beschreibungen/Notizen
Knowledge on the temperature distribution in high pressure and temperature devices is important for the interpretation of data and can often not be obtained from experiments. Here, we report on the thermal characteristics of the most employed Paris-Edinburgh press assemblies for in-situ X-ray purposes using finite element calculations. The maximal horizontal T variations in the sample are found to be small and amount maximal 50 K at 2500 K. Temperature differences between the sample and the calibrant material are in the same order of magnitude only if the latter is placed well centred on the sample capsule. The present (pure thermal) calculations can only partly reproduce the discrepancies between experimentally determined input power to T relations (1000 K at 350 W) indicating that different deformation behaviours of assemblies may play a crucial role. Based on the obtained results we present an optimized assembly in terms of sample temperature and gradients.