Details

Autor(en) / Beteiligte

• Shi, Songjie
• Wan, Li
• Sun, Xiaoning
• Zhang, Jiawei
• Guo, Kai

Titel

Methoxylation and Direct Hydrogenative Coupling of Chloronitrobenzenes in Continuous Flow

Ist Teil von

• Chinese journal of chemistry, 2017-04, Vol.35 (4), p.410-414

Ort / Verlag

Weinheim: WILEY-VCH Verlag GmbH & Co. KGaA

Erscheinungsjahr

2017

Quelle

Alma/SFX Local Collection

Beschreibungen/Notizen

• A novel continuous flow method for the methoxylation of chloronitrobenzenes was developed. The reaction went smoothly and high yields were achieved under the optimized conditions. Furthermore, up to 76% yield of azoxybenzenes were obtained from the corresponding nitrobenzenes in the presence of NaOH in continuous flow. Compared to batch conditions, the reaction time was significantly shortened, and the chemical waste was reduced obviously.