Details

Autor(en) / Beteiligte

• Fossey, John S
• Anslyn, Eric V
• Brittain, William D. G
• Bull, Steven D
• Chapin, Brette M
• Le Duff, Cécile S
• James, Tony D
• Lees, Glenn
• Lim, Stephanie
• Lloyd, Jennifer A. C
• Manville, Charles V
• Payne, Daniel T
• Roper, Kimberley A

Titel

Rapid Determination of Enantiomeric Excess via NMR Spectroscopy: A Research-Informed Experiment

Ist Teil von

• Journal of chemical education, 2017-01, Vol.94 (1), p.79-84

Ort / Verlag

Easton: American Chemical Society and Division of Chemical Education, Inc

Erscheinungsjahr

2017

Quelle

Alma/SFX Local Collection

Beschreibungen/Notizen

• An undergraduate chemistry experiment that draws from primary research is described. The experiment exploits chiral supramolecular assemblies for the determination of enantiomeric excess by 1H NMR spectroscopy. This report describes the delivery of the experiment to a cohort of students, and as a result of feedback from those involved, an optimized protocol is presented. Particular care has been taken to facilitate ready adoption in other institutions by providing comprehensive teaching support materials as well as technical guidance for supporting the experiment.