Journal of solid state chemistry, 2007-09, Vol.180 (9), p.2625-2629
2007
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Details
- Autor(en) / Beteiligte
- Titel
- Continuous nanoparticle production by microfluidic-based emulsion, mixing and crystallization
- Ist Teil von
- Journal of solid state chemistry, 2007-09, Vol.180 (9), p.2625-2629
- Ort / Verlag
- San Diego, CA: Elsevier Inc
- Erscheinungsjahr
- 2007
- Quelle
- Alma/SFX Local Collection
- Beschreibungen/Notizen
- BaSO 4 and 2,2′-dipyridylamine (DPA) nanoparticles were synthesized as reactive crystallization and anti-solvent recrystallization examples, respectively, of using the microfluidic-based emulsion and mixing approach as a new avenue of continuously producing inorganic and organic nanoparticles. BaSO 4 nanoparticles in the size range of 15–100 nm were reactively precipitated within the confinement of an aqueous droplet which was coalesced from two separate aqueous droplets containing BaCl 2 and (NH 4) 2SO 4 using a three T-junction micromixer configuration constructed with commercially available simple tubing and fitting supplies. Also, DPA nanoparticles of about 200 nm were crystallized by combining DPA+ethanol and water droplets using the same micromixer configuration. BaSO 4 and 2,2′-dipyridylamine (DPA) nanoparticles were synthesized as reactive crystallization and anti-solvent recrystallization examples, respectively, of using the microfluidic-based emulsion and mixing approach as a new avenue of continuously producing inorganic and organic nanoparticles.
- Sprache
- Englisch
- Identifikatoren
- ISSN: 0022-4596eISSN: 1095-726XDOI: 10.1016/j.jssc.2007.06.033Titel-ID: cdi_osti_scitechconnect_21043849
- Format
- –
- Schlagworte
- AMINES, AMMONIUM SULFATES, BARIUM CHLORIDES, BARIUM SULFATES, Chemical synthesis methods, Condensed matter: structure, mechanical and thermal properties, Cross-disciplinary physics: materials science, rheology, CRYSTALLIZATION, Emulsion, Equations of state, phase equilibria, and phase transitions, Exact sciences and technology, INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY, Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties, Materials science, Methods of nanofabrication, Microfluidics, Microreactor, Nanoparticles, Nanoscale materials and structures: fabrication and characterization, NANOSTRUCTURES, Other topics in nanoscale materials and structures, Physics, PYRIDINES, RECRYSTALLIZATION, Solid-solid transitions, Specific phase transitions, Surfaces and interfaces, thin films and whiskers (structure and nonelectronic properties)