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Control of Particle Characteristics in the Preparation of TiO2 Nano Particles Assisted by Microwave
Ist Teil von
Bulletin of the Korean Chemical Society, 2012, 33(5), , pp.1699-1702
Ort / Verlag
대한화학회
Erscheinungsjahr
2012
Quelle
EZB Electronic Journals Library
Beschreibungen/Notizen
TiO2 nanostructures with various morphologies like cubes, spheres, hexahedral pillars and spherical tubes were synthesized by microwave-assisted hydrothermal process. Each structure was obtained by changing the relative concentrations of titanium tetraisoproxide (TTIP), tetrabutylammonium hydroxide (TBAH) and ethanol. Scanning electron microscopy (SEM), transmission electoron microscopy (TEM), X-ray diffraction and Brunauer-Emmett-Teller (BET) surface area analysis were used to characterize the synthesized TiO2 nanostructures. From these results, it has been proved that TiO2 structure could be controlled to have specific morphology, size, surface area, pore volume and pore size distribution. KCI Citation Count: 8