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This article focuses on three recent applications of microwave and millimeter wave NDT&E techniques that involve novel instrumentation development and measurements, including: 1) disbond detection in strengthened concrete bridge members retrofitted with carbon fiber reinforced polymer (CFRP) composite laminates; 2) corrosion and precursor pitting detection in painted aluminum and steel substrates; and 3) detection of flaws in spray-on foam insulation and the acreage heat tiles of the Space Shuttle through focused and synthetic imaging techniques. These applications have been performed at the Applied Microwave Nondestructive Testing Laboratory (amntl) at the University of Missouri-Rolla.