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The investigation was aimed at developing procedures for the pharmaceutical analysis and standardization of the new domestic anxiolytic afobazole in solid dosage form (tablets). The main pharmacopoeial tests have been carried out and methods for the determination (TLC, HPLC), identification (TLC, UV spectrophotometry), and quantitative assay (UV spectrophotometry, HPLC) have been worked out. The test for uniformity of composition and the dissolution test were carried out with the aid of UVspectrophotometry.