Details

Autor(en) / Beteiligte

• Nishiyama, Yusuke
• Duong, Nghia Tuan

Titel

Practical guides for 1H detected solid-state NMR under fast MAS for small molecules

Ist Teil von

• Journal of Magnetic Resonance Open, 2022-06, Vol.10-11, p.100062, Article 100062

Ort / Verlag

Elsevier Inc

Erscheinungsjahr

2022

Quelle

Free E-Journal (出版社公開部分のみ）

Beschreibungen/Notizen

• •Practical guide to setup 1H detected solid-state NMR for small molecules under fast MAS is provided.•Basic setup of a fast MAS probe is demonstrated.•Experimental setup together with brief explanation of basic 1D and 2D experiments are demonstrated. This primer article introduces a practical guide for setting up 1H detection solid-state NMR experiments under fast MAS conditions for small molecules. Sample independent adjustment/calibration including magic angle adjustment, shimming, radio-frequency field calibration, Hartmann-Hahn matching adjustments, and 1H heteronuclear decoupling are demonstrated. Experimental setups which depend on samples are also shown for 1H NMR, 1H-1H homonuclear correlation measurements, and 1H-X heteronuclear correlation/distance measurements. Information obtained from each experiment is also highlighted. [Display omitted]