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In this study, in order to find novel biologically active pyrazole oxime derivatives, twenty-eight new pyrazole oxime compounds containing a substituted isoxazole ring were synthesized and evaluated for their acaricidaland insecticidal activities. Bioassays exhibited that some target compounds indicated good acaricidal and insecticidal activities against
,
,
, and
. Especially, compounds
,
,
, and
showed 100.00%, 90.56%, 90.78%, and 90.62% insecticidal activities against
at the concentration of 20 μg/mL, respectively, compounds
and
had 70.86% and 100.00% insecticidal activities against
at 20 μg/mL, respectively.