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Effects of γ-irradiation on AC electrical and impedance spectroscopy of Ni-Zn nano ferrites
Ist Teil von
Physica scripta, 2022-09, Vol.97 (9), p.95702
Ort / Verlag
IOP Publishing
Erscheinungsjahr
2022
Quelle
Alma/SFX Local Collection
Beschreibungen/Notizen
Abstract
Herein we report the effect of
γ
-irradiation on the structural and AC electrical properties of Ni-Zn nanoparticles
N
i
1
−
x
Z
n
x
F
e
2
O
4
0
≤
x
≤
1
synthesised via the citrate auto-combustion technique. The x-ray diffraction (XRD) analysis of the samples revealed a decreasing trend of the crystallite size with increasing concentration of Zn
2+
ions, and -irradiation alters the crystallite size for more Ni
2+
ion concentrations. The lattice constant was found to increase with Zn
2+
concentration, with the highest for x = 0.6. However, after irradiation, substantial change occurs. The lattice strain is greater for x = 1 as well as lower for x = 0.4. The observable modifications in the morphology of the samples upon irradiation are identified. The AC-electrical behaviour of the sample was studied before and after
γ
-irradiation in the frequency range of 1 MHz–23 MHz. Studies show that the dielectric constant increases on irradiation, whereas the dielectric loss and AC conductivity decline after irradiation. The dielectric relaxation changes from non-Debye to Havriliak–Negami relaxation, which is the significance of asymmetric broadness in the relaxation process. The collective AC electrical properties were signifies the radiation absorption response.