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Cellulose fibers isolated from energycane bagasse using alkaline and sodium chlorite treatments: Structural, chemical and thermal properties
Ist Teil von
Industrial crops and products, 2015-12, Vol.76, p.355-363
Ort / Verlag
Elsevier B.V
Erscheinungsjahr
2015
Quelle
Access via ScienceDirect (Elsevier)
Beschreibungen/Notizen
[Display omitted]
•Isolation of cellulose fibers was made from energycane using a combined NaOH and NaClO2 treatment.•Most lignin and hemicelluloses were removed from treatment.•The average width of fiber reduced to 12±5μm.•The significant changing in crystallinity occurred.•Isolated lignocellulose fibers had a one-step pyrolysis.
Cellulose fibers were successfully extracted from energycane bagasse by using a combined NaOH and NaClO2 treatment. After the delignification process, most lignin and hemicelluloses were removed with a 27.4wt% yield of cellulose fibers, and the mean diameter of cellulose fibers decreased from 137±46 (raw fiber bundles) to 12±5μm (unpacked fibers). The crystallinity of cellulose fibers first decreased and then increased during the transformation from cellulose I to II, and it gradually decreased after a further NaClO2 treatment. The raw bagasse fibers showed a three-step pyrolysis process, while isolated cellulose fibers had a one-step pyrolysis process. NaClO2 treatment caused the reduction of cellulose thermal stability due to its acting on lignin and cellulose.