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Oxidative and catalytic polymerizations of DEBP (
p-diethynylbiphenyl) were investigated. The characterization of the reaction products, ox-PDEBP and c-PDEBP (originating from the oxidative and catalytic reactions respectively), was performed by means of i.r., XPS and t.g.-d.t.a. techniques. The different behaviour of ox-PDEBP and c-PDEBP in the presence of oxygen and humidity was examined. The variations of the electrical properties upon doping with FeCl
3 and I
2 are also reported.